郑 丽,周日海,张婉婷,张金凤,彭 伟,陈业高*.红姜花中黄酮的分离与鉴定[J].海南师范大学学报自科版,2024,37(1):70-74 |
红姜花中黄酮的分离与鉴定 |
Isolation and Identification of Flavonoids from Hedychium coccineum |
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DOI: |
中文关键词: 红姜花 化学成分 黄酮 |
英文关键词: Hedychium coccineum chemical constituent flavonoid |
基金项目:云南省高校药用活性分子结构多样性研究重点实验室资助项目;云南师范大学“大学生科研训练基金项目”
(KX2022022) |
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中文摘要: |
风干粉碎后的红姜花(Hedychium coccineum)根茎用工业甲醇浸提,甲醇浸提物用乙酸
乙酯-水萃取。采用多种分离技术(硅胶柱层析、Sephadex LH-20、RP-18柱层析、HPLC)分离乙酸
乙酯浸膏中的化学成分,通过NMR等方法对所得的化合物进行结构鉴定。共鉴定6个黄酮类化合
物,分别是 5-hydroxy-3,7,4’-trimethoxyflavone (1)、3,5-dihydroxy-7,4’-dimethoxyflavone (2)、
kaempferol-4’-O-methylether (3)、ermanin (4)、dihydrokaempferide (5)、aromadendrin-7,4'-dimethyl
ether (6)。均为首次从红姜花中分离得到。 |
英文摘要: |
The air-dried and crushed rhizomes of Hedychium coccineum were extracted with MeOH, and the extract was
partitioned with EtOAc-H2O. The EtOAc extract was isolated by various separation techniques (Silica gel, Sephadex LH-
20, RP-18 column chromatography and HPLC). By means of spectroscopic analysis, the isolated compounds were identi⁃
fied as 5-hydroxy-3,7,4'-trimethoxyflavone (1), 3,5-dihydroxy-7,4'-dimethoxyflavone (2), kaempferol-4'-O-methylether
(3), ermanin (4), dihydrokaempferide (5) and aromadendrin-7,4'-dimethyl ether (6). All the compounds were isolated from
H. coccineum for the first time. |
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