| 王朝训,罗 清,姚 静,谢志胥,陈业高*.姜花中二芳基庚烷及黄酮成分的分离鉴定[J].海南师范大学学报自科版,2022,35(2):133-136 |
| 姜花中二芳基庚烷及黄酮成分的分离鉴定 |
| Isolation and Identification of Diarylheptanoids and Flavonoids inHedychium coronarium Koen |
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| DOI:10.12051/j.issn.1674-4942.2022.02.004 |
| 中文关键词: 姜花 二芳基庚烷 黄酮 结构鉴定 |
| 英文关键词: Hedychium coronarium Koen diarylheptanoids flavonoids structure identification |
| 基金项目: |
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| 摘要点击次数: 1111 |
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| 中文摘要: |
| 姜花( Hedychium coronarium Koen)根茎用甲醇提取,利用硅胶柱层析、Sephadex LH-20
柱层析、薄层层析及HPLC等手段对其化学成分进行分离纯化,得到5个化合物,经波谱解析和对
其理化性质进行对比,鉴定为3个二芳基庚烷和2个黄酮,分别是gingerenone A(1 1),rel-(3 R ,5 S )-3,
5-dihydroxy-1-(4-hydroxy-3-methoxyphenyl)-7-(4-hydroxyphenyl)-heptane(2 2),hexahydrocurcumin
(3 3),3,5,7,4´-tetramethoxyflavone(4 4)和5-hydroxy-3,7,4´-trimethoxyflavone(5 5)。化合物1 1~4 4为
首次从姜花中分离得到。 |
| 英文摘要: |
| Five compounds were isolated from the methanol extract of the rhizomes of Hedychium coronarium Koen by sili⁃
ca gel column chromatography, Sephadex LH-20 chromatography, thin layer chromatography and high performance liquid
chromatography. Their structures were identified by spectroscopic analysis combined with their physicochemical data.
Three diarylheptanes and two flavonoids were identified as gingerenone A (1), rel-(3R,5S)-3,5-dihydroxy-1-(4-hydroxy-
3-methoxyphenyl)-7-(4-hydroxyphenyl)-heptane (2), hexahydrocurcumin (3), 3,5,7,4´-tetramethoxyflavone (4) and 5-hy⁃
droxy-3,7,4´-trimethoxyflavone (5). Compounds 1~4 were isolated from this plant for the first time. |
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